Cryostat-500
instrumentation
Cryostat-500 (KSC-TOPS-43)
Thermal Insulation Test Apparatus
Overview
NASA Kennedy Space Center seeks partners interested in the guarded flat plate insulation test cryostat (Cryostat-500), a boil-off calorimeter comprised of a flat bottom test apparatus for measuring the absolute thermal performance of an insulation test specimen. This instrument provides convenient testing of many sizes and shapes of materials, enhanced automation, and a direct route for obtaining reliable thermal performance data. Testing under conditions representative of actual-use environments including large temperature differences is also provided. The test data are presented in terms of effective thermal conductivity and heat flux.
In today's world, efficient, low-maintenance, low-temperature refrigeration is taking a more significant role, from the food industry, transportation, and medical applications to commercial buildings, energy, and space exploration. Worldwide, various regulations require that commercially available insulation materials are tested and evaluated by an accepted methodology. The new Cryostat-500 method goes beyond the prior capabilities of consensus technical standards to provide testing for real systems and materials operating below ambient temperature. The Cryostat-500 covers a wide range of test environments including full-temperature differences plus full-range vacuum conditions.
The Technology
The Cryostat-500 provides laboratory measurement of the steady-state thermal transmission properties of thermal insulation systems under conditions below ambient temperature. Liquid nitrogen is used as a direct measure of the energy going through the test specimen. Thermal insulation systems may be composed of one or more materials that may be homogeneous or non-homogeneous at boundary conditions from 77 K to 373 K and in environments from high vacuum (10E-7 torr) to ambient pressure (10E+3 torr).
The Cryostat-500 provides a much wider range of thermal performance and covers the full range of environmental conditions for applications below ambient temperature. The instrument has been proven through extensive testing of foams, composite panels, multilayer insulation (MLI) systems, aerogel blankets, fiberglass, and many other types of materials. Both the quality and quantity of the thermal performance data for insulation materials and systems have increased even as the process and method has become more time efficient and cost effective. Further guidelines on the test method and equipment for the Cryostat-500 are given in ASTM C1774, Annex A3.
Benefits
- Provides a wider range of heat flux performance
- Allows testing over the full range of environmental conditions
- Proven through extensive testing of hundreds of insulation systems and materials
- Increased quality and quantity of thermal performance data
- Cost effective and time efficient
Applications
- Electrical power generation and transmission
- Refrigeration and HVAC
- Ground and air transportation (e.g., refrigerated transport)
- Medical equipment
- Food processing
- Electronics manufacturing
- Aerospace
- Architecture and construction
- Multiple energy-related industries and sectors
- Cryogenic storage, transport, and distribution, including LNG and LH2
Tags:
|
Similar Results
Cryostat-100
Cryostat-100 combines the best features of previous cryostats developed by NASA, while offering new features and conveniences. This unit can readily handle the full range of cryogenic-vacuum conditions over several orders of magnitude of heat flux. Guide rings, handling tools, and other design items make insulation change-out and test measurement verification highly reliable and efficient to operate. The new apparatus requires less ancillary equipment (it is not connected to storage tank, phase separator, subcooler, etc.) to operate properly. It is top-loading, which makes disassembly, change-out, and instrumentation hook-up much faster. The thermal stability is improved because of internal vapor plates, a single-tube system of filling and venting, bellows feed-throughs, Kevlar thread suspensions, and heavy-wall stainless-steel construction.
The cold mass of Cryostat-100 is 1m long, with a diameter of 168 mm. The test articles can therefore be of a corresponding length and diameter, with a nominal thickness of 25.4 mm. Shorter lengths are acceptable, and thicknesses may be from 0 mm to 50 mm. Tests are conducted from ambient pressure (760 torr) to high vacuum (below 110-4 torr) and at any vacuum pressure increment between these two extremes. The residual gas (and purge gas) is typically nitrogen but can be any purge gas, such as helium, argon, or carbon dioxide.
Typically, eight cold vacuum pressures are performed for each test series. The warm boundary temperature is approximately 293 K, and the cold boundary temperature is approximately 78 K. The delta temperature for the cryogenic testing is therefore approximately 215 K. A unique lift mechanism provides for change-out of the insulation test specimens. It also provides for maintenance and other operations in the most effective and time-efficient ways. The lift mechanism is also a key to the modularity of the overall system.
Macroflash (Cup Cryostat)
Advances in new polymers and composites along with growing industrial needs in below-ambient temperature applications have brought about the Macroflash development. Accurate thermal performance information, including effective thermal conductivity data, are needed under relevant end-use conditions. The Macroflash is a practical tool for basic testing of common materials or research evaluation of advanced materials/systems.
The Macroflash can test solids, foams, or powders that are homogeneous or layered in composition. Test specimens are typically 75mm in diameter and 6mm in thickness. The cold side is maintained by liquid nitrogen at 77 K while a heater disk maintains a steady warm-side temperature from ambient up to 373 K. The steady boiloff of the liquid nitrogen provides a direct measure of the heat energy transferred through the thickness of the test specimen. Nitrogen or other gas is supplied to the instrument to establish a stable, moisture-free, ambient pressure environment. Different compression loading levels can also be conveniently applied to the test specimen as needed for accurate, field-representative thermal performance data. The Macroflash is calibrated from approximately 10 mW/m-K to 800 mW/m-K using well-characterized materials.
Li-ion Cell Calorimeter
Li-ion batteries are an integral part of energy storage systems used in NASA's Exploration program, as well as many modern terrestrial industries. Innovators at the NASA Johnson Space Center wanted a better way to measure total and fractional heat response of specific types of Li-ion cells when driven into a thermal runaway condition. They developed a calorimeter with at least two chambers, one for the battery cell under test and at least one other chamber for receiving the thermal runaway ejecta debris. Both are designed to be structurally strong and thermally insulated. When the test cell is intentionally driven into thermal runaway, ejecta explodes into the ejecta chamber and is decelerated and collected. Thermal sensors are strategically placed throughout the chambers to collect thermal data during the test. Customized software analyzes the thermal data and determines key calorimeter parameters with a high degree of accuracy.
Thin Film Sensor for Ultra High-Temp Measurement
The thin film sensor’s principal advantage lies in its potential to take high frequency temperature measurements from the surface of a reentering spacecraft while simultaneously withstanding the high temperature and oxidizing environment encountered. This data provides engineers with operational phase measurements used to refine the spacecraft’s operational envelope and track flight hardware behavior in addition to providing high frequency temperature measurements that can inform the physics of a boundary layer.
Mismatches in coefficients of thermal expansion (CTE) are expected in TPS-based sensor applications because the metallic materials used for temperature sensing have thermal expansion rates that differ from the rates of the substrate and coating materials in the TPS. At high temperatures during reentry, this mismatch in CTE can create a significant strain differential between the metallic sensor, sensor leads, and the materials to which the sensor and leads are bonded.
High frequency response temperature measurements on the surface of entry spacecraft are not currently possible above ~700 F with existing measurement capabilities. This shortcoming is primarily due to the need for robust sensor behavior at temperatures of several thousand degrees F. The sensor design of this technology preserves the integrity of sensor components while enhancing its high temperature functionality.
The thin film temperature sensor has a technology readiness level (TRL) 5 (Component and/or breadboard validation in relevant environment) and is now available for patent licensing. Please note that NASA does not manufacture products itself for commercial sale.
Multilayered Fire Protection System
The Multilayered Fire Protection system uses technology from the space craft flexible heat shield for future planetary missions. By optimizing this material for the fire environment, utilizing heat shield test methods, and experimenting with different materials, the NASA team developed a multilayered fire protection system. This system includes an outer textile layer which reflects over 90 percent of the radiant heat, an insulated layer which protects against convective heat and hot gases, and a non-porous film layer which is a gas barrier layer.